Showing posts with label Nordihydroguaiaretic acid Suppliers. Show all posts
Showing posts with label Nordihydroguaiaretic acid Suppliers. Show all posts

Monday, January 6, 2014

Identification of Nordihydroguaiaretic acid test



Solubility Nordihydroguaiaretic acid soluble in ethanol and ethyl ether, soluble in 116 ℃ propylene glycol. According to the OT - 42 method determination.
Determination of melting point 184 ℃, according to the conventional method.
Take ferric chloride ethanol solution (TS - 102) 12 ml and 2, 2 pyridine test solution (TS - 41) 2 ml, add 50% ethanol solution containing 0.5% sample 5 ml, should be dark fuchsia.
Take a sample liquid 5 ml 75% ethanol, 1% with concentrated ammonia solution (TS - 13) 1 ml, should be yellow.
Take sample liquid 10 ml 50% ethanol, 0.5% and 1% barium hydroxide [Ba (OH) 2? H2O3 boiling liquid 1.5 ml. Should be dark blue, and can keep about 1 h.
Take 10% sodium hydroxide 10 ml, add 0.5% sample


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